[Inorganic Syntheses] Inorganic Syntheses (Rochow/Inorganic) || Trisodium Trimetaphosphimate 1-Hydrate

✍ Scribed by Rochow, Eugene G.

• Book ID: 102682165
• Publisher: John Wiley & Sons, Inc.
• Year: 2007
• Weight: 693 KB
• Category: Article
• ISBN: 0470131659
• DOI: 10.1002/9780470132371.ch30

✦ Synopsis

The hydrolysis of trimeric phosphonitrile chloride dissolved in ether and shaken with aqueous sodium acetate solution was described by St0kes.l It is slow and uncertain, however, and the substitution of dioxane for ether, as practiced by de Fiequelmont in related preparations, is preferred.