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Infrared study of complexes between iron, salicylaldehyde benzoyl hydrazone and seven analogous derivatives

✍ Scribed by Cosima Colonna; Jean-Pierre Doucet; Aliette Cossé-Barbi


Publisher
Springer
Year
1995
Tongue
English
Weight
483 KB
Volume
20
Category
Article
ISSN
0340-4285

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✦ Synopsis


An i.r. study of Fe complexes prepared from salicylaldehyde benzoyl hydrazone and seven similar chelating agents allowed the assignment of some iron-ligand bands. The amide I and ~b--O band shifts indicate that the ligand O atoms are directly linked to Fe. The analogy between FdI and Fe In complexes in the mid-i.r, range and the chiefly identical frequencies in the far-ix, range provide evidence that oxidation of Fe II has occurred. The bands directly involved in complexation are shifted compared to the free hydrazones, and all are medium or weak.