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Infrared Spectroscopy of Fragments from Doubly Protonated Tryptic Peptides

✍ Scribed by Benjamin J. Bythell; Undine Erlekam; Béla Paizs; Philippe Maître


Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
201 KB
Volume
10
Category
Article
ISSN
1439-4235

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✦ Synopsis


Abstract

Most proteins in proteomics are identified from tandem mass spectra of doubly protonated tryptic peptides. Statistical studies indicate that these spectra fall into two distinct classes. IR spectroscopy experiments and DFT calculations performed on model b~2~ ions show that peptides producing Class I spectra form protonated oxazolone ions (see figure) and not protonated diketopiperazines as proposed elsewhere.magnified image