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Infrared and Raman spectra, conformations, ab initio calculations and spectral assignments of 1-fluoro-1-silacyclohexane

✍ Scribed by Peter Klaeboe; Valdemaras Aleksa; Claus J. Nielsen; Anne Horn; Gamil A. Guirgis; Michael D. Johnston

Book ID
113806295
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
580 KB
Volume
1015
Category
Article
ISSN
0022-2860

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## Abstract Raman spectra of 1,3‐disilabutane (SiH~3~CH~2~SiH~2~CH~3~) as a liquid were recorded at 293 K and as a solid at 78 K. In the Raman cryostat at 78 K an amorphous phase was first formed, giving a spectrum similar to that of the liquid. After annealing to 120 K, the sample crystallized and