Influencing the satellite transitions of half-integer quadrupolar nuclei for the enhancement of magic angle spinning spectra
✍ Scribed by Dinu Iuga; Arno P.M Kentgens
- Book ID
- 108487759
- Publisher
- Elsevier Science
- Year
- 2002
- Tongue
- English
- Weight
- 281 KB
- Volume
- 158
- Category
- Article
- ISSN
- 1090-7807
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## Abstract A comprehensive experimental and numerical study of the potential of fast amplitude (FAM) irradiation for improving the triple‐quantum (3Q) magic angle spinning (MAS) NMR spectra of half‐integer $I > {1 \over 2}$ nuclei (^23^Na, ^27^Al, ^45^Sc, ^93^Nb) was carried out. Materials of acad
## Abstract Variable‐angle sample‐spinning (VASS) NMR was investigated for the case of limited rotation speed of the spinner. Side‐band intensities and line‐shapes for the central transition of half‐integer quadrupolar spin nuclei were calculated as a function of the parameter \documentclass{articl