## Abstract **BACKGROUND:** The influence of technological parameters on the epoxidation of 1‐butene‐3‐ol (1B3O) over titanium silicalite TS‐2 catalyst has been investigated. Epoxidations were carried out using 30%(w/w) hydrogen peroxide at atmospheric pressure. The major product from the epoxidati
Influence of process parameters on the epoxidation of 2-buten-1-ol over titanium silicalite TS-1 catalyst
✍ Scribed by Agnieszka Wróblewska; Ewelina Ławro; Eugeniusz Milchert
- Book ID
- 111491118
- Publisher
- Versita
- Year
- 2008
- Tongue
- English
- Weight
- 299 KB
- Volume
- 62
- Category
- Article
- ISSN
- 0366-6352
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✦ Synopsis
Abstract
The influence of process parameters on the epoxidation of 2-buten-1-ol with 30 % hydrogen peroxide using the titanium silicalite TS-1 is presented. The studies were carried out under autogenic pressure (in autoclave). Methanol was used as a solvent in this process. The influence of temperature, 2-buten-1-ol to hydrogen peroxide mole ratio, amount of solvent used, TS-1 catalyst content, and reaction time on the reaction was studied. The major product of this reaction, 2,3-epoxybutan-1-ol (EB), has numerous applications in chemical industry.
📜 SIMILAR VOLUMES
## Abstract Titanium silicalite‐1 (TS‐1) films were prepared on SiO~2~ pellet supports via an __in situ__ hydrothermal synthesis method and were characterized by X‐ray diffraction (XRD), Fourier transform infrared spectroscopy (FT‐IR), scanning electron microscopy (SEM) and ^29^Si magic angle spinn