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Influence of process parameters on the epoxidation of 2-buten-1-ol over titanium silicalite TS-1 catalyst

✍ Scribed by Agnieszka Wróblewska; Ewelina Ławro; Eugeniusz Milchert


Book ID
111491118
Publisher
Versita
Year
2008
Tongue
English
Weight
299 KB
Volume
62
Category
Article
ISSN
0366-6352

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✦ Synopsis


Abstract

The influence of process parameters on the epoxidation of 2-buten-1-ol with 30 % hydrogen peroxide using the titanium silicalite TS-1 is presented. The studies were carried out under autogenic pressure (in autoclave). Methanol was used as a solvent in this process. The influence of temperature, 2-buten-1-ol to hydrogen peroxide mole ratio, amount of solvent used, TS-1 catalyst content, and reaction time on the reaction was studied. The major product of this reaction, 2,3-epoxybutan-1-ol (EB), has numerous applications in chemical industry.


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