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Inexpensive Protocol for Reduction of Imines to Amines Using Polymethylhydrosiloxane (PMHS)

โœ Scribed by Chandrasekhar, S.; Reddy, M. Venkat; Chandraiah, L.

Book ID
111885980
Publisher
Taylor and Francis Group
Year
1999
Tongue
English
Weight
265 KB
Volume
29
Category
Article
ISSN
0039-7911

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A mild, convenient, and inexpensive meth
A mild, convenient, and inexpensive method for converting imines into amines: Tin-catalyzed reduction with polymethylhydrosiloxane (PMHS)
โœ Rosa M. Lopez; Gregory C. Fu ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 338 KB

We have developed a mild, convenient, and inexpensive protocol for reducing imines to amines. Thus, treatment of any of a wide array of imines with catalytic n-butyltris(2-ethylhexanoate)tin and stoichioimetric polymethylhydrosiloxane (PMHS) in ethanol at room temperature cleanly affords the desired