In Situ XAS and XRD Studies on the Formation of Mo Suboxides during Reduction of MoO3†
✍ Scribed by Ressler, T.; Jentoft, R. E.; Wienold, J.; Günter, M. M.; Timpe, O.
- Book ID
- 111869180
- Publisher
- American Chemical Society
- Year
- 2000
- Tongue
- English
- Weight
- 373 KB
- Volume
- 104
- Category
- Article
- ISSN
- 0022-3654
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
## Abstract The bulk structural evolution during the decomposition of ammonium paratungstate (APT) under various oxidizing and reducing gases was elucidated by the complementary techniques, in situ XAS, in situ XRD, and TG/DSC, combined with mass spectrometry. In the temperature range from 300 to 6
We report a detailed in situ study of the preparation of the -phase Bi 2 MoO 6 catalyst from a gel. In particular, the local coordination around molybdenum remained tetrahedral, although the poorly crystalline bismuth molybdate phase started to appear below 4003C; above this temperature there was a