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In-situ Synchrotron X-ray Diffraction Study of the Formation of Cubic Li2TiO3 Under Hydrothermal Conditions

✍ Scribed by Andreas Laumann; Kirsten Marie Ørnsbjerg Jensen; Christoffer Tyrsted; Martin Bremholm; Karl Thomas Fehr; Michael Holzapfel; Bo Brummerstedt Iversen


Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
314 KB
Volume
2011
Category
Article
ISSN
1434-1948

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A continuous process for the synthesis of mesoporous silicates such as MCM-41 at room temperature has been achieved by employing a tubular reactor in which tetraethoxysilane was used as the silicate source (see schematic representation below). The formation of the hexagonal mesophase, which was moni