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In situ preparation of disulfide by the reaction of trialkyl- and triarylborons with sulfur

โœ Scribed by Zen-ichi Yoshida; Tsuneo Okushi; Osamu Manabe


Book ID
104248902
Publisher
Elsevier Science
Year
1970
Tongue
French
Weight
114 KB
Volume
11
Category
Article
ISSN
0040-4039

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The sulfur vulcanization of polyisoprene accelerated by 2-bisbenzothiazole-2,2'-disulfide (MBTS) was investigated. Rubber compounds were heated in a DSC and removed at various temperatures along the DSC thermal curve. The rubber vulcanizate was analyzed for crosslink density and for residual reactan