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In situ NMR of heterogeneous catalysis: new methods and opportunities

โœ Scribed by James F. Haw


Book ID
110385612
Publisher
Springer
Year
1999
Tongue
English
Weight
98 KB
Volume
8
Category
Article
ISSN
1022-5528

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The temperature of zeolite samples containing adsorbed methanol molecules was switched from room temperature to 500-600 K within 30-40 s by means of a laser beam. The catalytic reaction was monitored by 13C MAS NMR and 'H MAS NMR, the latter in steps of one second. A two-dimensional Fourier-transfor