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In situ FTIR study of the formation of MCM-41

✍ Scribed by Holmes, Stuart M.; Zholobenko, Vladimir L.; Thursfield, Alan; Plaisted, Richard J.; Cundy, Colin S.; Dwyer, John


Book ID
120037892
Publisher
Royal Society of Chemistry
Year
1998
Tongue
English
Weight
320 KB
Volume
94
Category
Article
ISSN
0956-5000

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A continuous process for the synthesis of mesoporous silicates such as MCM-41 at room temperature has been achieved by employing a tubular reactor in which tetraethoxysilane was used as the silicate source (see schematic representation below). The formation of the hexagonal mesophase, which was moni