𝔖 Bobbio Scriptorium
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In-Phase Selective Excitation of Overlapping Multiplets

✍ Scribed by Graham J Harris; Sarah R Lowe; Timothy J Norwood

Book ID
102600333
Publisher
Elsevier Science
Year
2000
Tongue
English
Weight
68 KB
Volume
142
Category
Article
ISSN
1090-7807

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✦ Synopsis

An editing experiment is presented that selects for a peak on the basis of its chemical shift and that of one of its scalar coupling partners. The selected multiplet is pure in-phase. The editing procedure can be used in conjunction with 1D TOCSY/ HOHAHA and NOE measurements. The pulse sequence described is particularly suitable for small molecules; data is presented for Gramicidin S and dehydrotestosterone.

πŸ“œ SIMILAR VOLUMES

Selective excitation of overlapping mult
Selective excitation of overlapping multiplets; the application of doubly selective and chemical shift filter experiments to complex NMR spectra
✍ Sara J. Duncan; Richard Lewis; Michael A. Bernstein; Peter Sandor πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 205 KB πŸ‘ 1 views

## Abstract Standard 1D TOCSY and NOE experiments have limitations where signals are severely overlapped. Here, two recently published selective excitation methods are evaluated, the first of which uses a chemical shift selective filter to select a single resonance based on its chemical shift, and