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Improved Synthesis of Oligodeoxyribonucleotides by Solid-Phase Phosphotriester Method Utilizing O6-[2-(p-Nitrophenyl)ethyl]-2′-deoxyguanosine Derivatives

✍ Scribed by André Chollet; Edgar Ayala; Eric H. Kawashima


Publisher
John Wiley and Sons
Year
1984
Tongue
German
Weight
610 KB
Volume
67
Category
Article
ISSN
0018-019X

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✦ Synopsis


Abstract

The synthesis of oligodeoxyribonucleotides on a cross‐linked polystyrene solid support utilizing stable mono‐ and dinucleotide phosphotriester building blocks is presented. The use of O^6^[2‐(p‐nitrophenyl)ethyl]‐2′‐deoxyguanosine derivatives yields cleaner DNA fragments by suppressing side reactions. Modifications improving the phosphotriester methodology are presented. The purification methods and analysis of synthetic oligodeoxyribonucleotides are described.