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Improved synthesis of 6,6,7,7-tetramethyl-1-azabicyclop[2.2.2]octan-2-one and its stability toward base-induced methanolysis

โœ Scribed by Arthur Greenberg; Guanli Wu; Jung-Chou Tsai; Yeu-Yi Chiu


Book ID
104882094
Publisher
Springer
Year
1993
Tongue
English
Weight
253 KB
Volume
4
Category
Article
ISSN
1040-0400

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## Abstract We report herein a reliable synthesis of P(OCH~2~)~3~P in a study aimed at understanding the factors that control its formation. We also report the serendipitous synthesis of the novel phosphiranol (CH~2~)~2~PO~2~H and the synthesis of P(PhNCH~2~)~3~P in good yield. ยฉ 2001 John Wiley &