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Improved synthesis and purification of methylated amanitins using diazomethane*

✍ Scribed by LITTLE, MICHAEL C. ;PRESTON, JAMES F. ;BONETTI, SANDRA

Book ID
115098514
Publisher
Wiley (Blackwell Publishing)
Year
2009
Tongue
English
Weight
444 KB
Volume
28
Category
Article
ISSN
0367-8377

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## Abstract A 20 mmole quantity of methyl‐^13^C fluoride at a ^13^C‐enrichment level of 90% was prepared by a two‐step synthesis starting with methanol‐^13^C. The overall yield was 60% of methanol used. A series of gas‐chromatographic treatments using Ascarite, silica gel, and Chromosorb‐102 column