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Improved Procedure for the Reductive Intermolecular Cyclodehalogenation of 2,6-Dibromocyclohexanones to Furan and Fulvenes

✍ Scribed by Schottelius, Thilo ;Hoffmann, H. Martin R.


Book ID
101817356
Publisher
Wiley (John Wiley & Sons)
Year
1991
Tongue
English
Weight
275 KB
Volume
124
Category
Article
ISSN
0009-2940

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## Abstract A method for the nitration of benzo‐2,1,3‐selenadiazoles using nitric acid dissolved in a mixture of methanesulfonic acid and phosphorus pentoxide at room temperature is presented. The S~N~2Ar displacement of fluoride that is observed when sulfuric acid is used as solvent is prevented a