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Improved method for the preparation of TiN-coated WC-Co-based samples for cross-sectional AEM investigation

✍ Scribed by J. Hefter; K. Ostreicher; C. Sung


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
440 KB
Volume
23
Category
Article
ISSN
1059-910X

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✦ Synopsis


Abstract

An improved method for the preparation of cross‐sectional thin foils of coated WC‐Co samples for studies by analytical electron microscopy is described. A braze alloy is used to join the sections of the sample together and the resulting sample is stable during subsequent grinding, dimpling, and milling operations. Cross‐sectional micrographs provide examples of the efficacy of this method. No microstructural alteration associated with the brazing operation was observed. © 1992 Wiley‐Liss, Inc.