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Identification of oxazepam and lorazepam glucuronides by chemical ionization mass spectrometry

โœ Scribed by T. T. L. Chang; Ch. F. Kuhlman; R. T. Schillings; S. F. Sisenwine; C. O. Tro; H. W. Ruelius

Book ID
112657516
Publisher
Springer
Year
1973
Tongue
English
Weight
342 KB
Volume
29
Category
Article
ISSN
1420-682X

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Gas chromatography/negative chemical ion
Gas chromatography/negative chemical ionization mass spectrometry of intact glucuronides
โœ Sharon Y. Brown; William A. Garland; Elaine K. Fukuda ๐Ÿ“‚ Article ๐Ÿ“… 1990 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 390 KB ๐Ÿ‘ 2 views

Gas chromatography-negative chemical ionization mass spectrometry (GC-NCIMS) has been applied to the analysis of 0-and S-glucuronides. The glucuronides were derivatized with pentafluorobenzyl (PFB) bromide and Tri-Sil, and analyzed by GC-NCIMS. All glucuronides gave a large [M-PFBI-ion indicative of