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Identification of Anomeric Configuration of Underivatized Reducing Glucopyranosyl-glucose Disaccharides by Tandem Mass Spectrometry and Multivariate Analysis

✍ Scribed by Simões, Joana; Domingues, Pedro; Reis, Ana; Nunes, Fernando M.; Coimbra, Manuel A.; Domingues, M. Rosário M.


Book ID
120159837
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
438 KB
Volume
79
Category
Article
ISSN
0003-2700

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## Abstract Negative‐ion electrospray mass spectrometry was used to determine directly both glycosidic linkage position and anomeric configuration in the complete glucopyranosyl disaccharide series without the need for derivatization or tandem mass analysis. A series of empirical criteria were deve