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Identification and characterization of solid-state nature of 2-chloromandelic acid

✍ Scribed by Quan He; Jesse Zhu; Hassan Gomaa; Michael Jennings; Sohrab Rohani


Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
316 KB
Volume
98
Category
Article
ISSN
0022-3549

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✦ Synopsis


The racemate and enantiomers of 2-chloromandelic acid were characterized by SS-NMR, XRPD, and FTIR. The binary melting point phase diagram was constructed by DSC (differential scanning calorimetry). The solid-state nature of 2-chloromandelic acid was identified to be a racemic compound. The crystal structure of racemic compound was determined to be monoclinic P2 1 /c.


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