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Hypervalent iodine oxidation: α-Functionalization of β-dicarbonyl compounds using iodosobenzene

✍ Scribed by Robert M. Moriarty; Radhe K. Vaid; Vasulinga T. Ravikumar; Beena K. Vaid; Thomas E. Hopkins

Publisher
Elsevier Science
Year
1988
Tongue
French
Weight
456 KB
Volume
44
Category
Article
ISSN
0040-4020

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Primary aliphatic amines on oxidation with iodosobenzene in CH2C12 or H20 yield the corresponding nitriles, while primary cycloalkylamines give the corresponding cyclic ketones. Lactams are obtained by the oxidation of cyclic amines. (S)(-) Nicotine (JJ,) is oxidized to (+)-cotinine (a). The interm