Hydroxymethylfuraldimines: Possible intermediates in maillard reaction

✍ Scribed by Robert H. Higgins

• Publisher: John Wiley and Sons
• Year: 1974
• Tongue: English
• Weight: 240 KB
• Volume: 63
• Category: Article
• ISSN: 0022-3549
• DOI: 10.1002/jps.2600631037

✦ Synopsis

Nu: R=C1, X=H v Ri=a X=Cl v a : R='CL x=cI was removed and the dark-yellow solution was allowed to stand for 0.5 hr. ThB reaction mixture was then poured into crushed ice and the solid material was collected and washed several times with water. Recrystallization from methanol gave crystals, mp 135- 137'. NMR analysis in acetone-ds gave a proton count of seven, showing the four protons for the benzene ring at 8 ppm and a singlet (three protons) a t 3.75 ppm for the methyl group in the 2-position.

Anal.-cak.