Hydroxyacetylene: Generation and Characterization of the Neutral Molecule, Radical Cation and Dication in the Gas Phase
β Scribed by Ben van Baar; Dr. Thomas Weiske; Dr. Johan K. Terlouw; Prof. Dr. Helmut Schwarz
- Publisher
- John Wiley and Sons
- Year
- 1986
- Tongue
- English
- Weight
- 319 KB
- Volume
- 25
- Category
- Article
- ISSN
- 0044-8249
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π SIMILAR VOLUMES
200 mL) was acidified with 3 drops of 32% HCI and stirred for 15 min at 50Β°C (exclusion of light). After extraction with CH,CI,, the organic phase was dried (Na,SO,) and purified on silica gel (20 8). After removal of the solvent there remained 0.53 g (72%) of a crystalline product. For further puri
processes has been described for the reactions of some halogen-1993). With respect to radical anions in the gas phase, a substituted carbene radical anions with the methyl ester of trifluoroacetic acid and dimethyl carbonate. The structural charac-more limited number of reports has appeared irrespec