Hydrothermal Synthesis of MoS2 and Its Pressure-Related Crystallization

✍ Scribed by Yiya Peng; Zhaoyu Meng; Chang Zhong; Jun Lu; Weichao Yu; Zhiping Yang; Yitai Qian

• Publisher: Elsevier Science
• Year: 2001
• Tongue: English
• Weight: 276 KB
• Volume: 159
• Category: Article
• ISSN: 0022-4596
• DOI: 10.1006/jssc.2001.9146

✦ Synopsis

Crystalline, poorly crystalline, and single-layer MoS 2 were synthesized using a hydrothermal method at low temperature (170+2003C) through changing pressure and time. XPS, XRD, and TEM were used to study the products. It was found that the stacking of the single layers was closely related to the pressure in the autoclave. A model was presented to explain this phenomenon.