Hydrothermal synthesis of [H3N(CH2)3NH3][V4O10]
β Scribed by Faouzi Sediri; Noureddine Etteyeb; Neji Gharbi; Nathalie Steunou; Jacques Livage
- Book ID
- 114124600
- Publisher
- Editions Lavoisier
- Year
- 2003
- Tongue
- English
- Weight
- 547 KB
- Volume
- 28
- Category
- Article
- ISSN
- 0151-9107
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A new layered vanadium oxide [H 3 N(CH 2 ) 4 NH 3 ](V 6 O 14 ) was synthesized hydrothermally under autogenous pressure at 1801C for 48 h from a mixture of H 2 N(CH 2 ) 4 NH 2 and V 2 O 5 in aqueous solution. Its structure was determined from singlecrystal X-ray diffraction at room temperature with
Die Hydrothermalchemie in Gegenwart von organischen strukturdirigierenden Agentien ist eine sehr vielseitige Technik zur Synthese neuer Schicht-und dreidimensionaler GerΓΌstmaterialien. Die Vielseitigkeit dieser Technik rΓΌhrt von der ausgezeichneten Kontrolle ΓΌber die genaue Topologie des anorganisc