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Hydrothermal synthesis and structure refinements of alkali-metal trivanadates AV3O8 (A = K, Rb, Cs)

✍ Scribed by Yoshio Oka; Takeshi Yao; Naoichi Yamamoto

Book ID
114066819
Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
611 KB
Volume
32
Category
Article
ISSN
0025-5408

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The synthesis and single-crystal structures of four alkali+ metal amalgams are reported. The compounds A 3 Hg 20 (A ‫؍‬ Rb, Cs) are of new structural type (Pm-3n, Z‫,2؍‬ a ‫؍‬ 10.737(1) A s and 10.913(1) A s , for A ‫؍‬ Rb and Cs, respectively), while K 3 Hg 11 is the 5rst example of a mercury compo