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Hydrothermal synthesis and structure of a molybdenum oxide (TMA)2[Ni(H2O)6][β-Mo8O26]

✍ Scribed by Sheming Lu; Yanxiong Ke; Jianmin Li; Yugen Zhang

Book ID
114370664
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
229 KB
Volume
5
Category
Article
ISSN
1293-2558

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Hydrothermal Synthesis and Structures of
Hydrothermal Synthesis and Structures of Two Tetramethylammonium Iron Molybdates (TMA)2FeMo6O20and [TMA]2[Fe(H2O)6]Mo8O26
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Two new compounds (TMA) 2 FeMo 6 O 20 and [TMA] 2 [Fe(H 2 O) 6 ]Mo 8 O 26 have been synthesized by hydrothermal reactions. (TMA) 2 FeMo 6 O 20 crystallizes in the monoclinic space group C2/m; a ‫؍‬ 21.204(1) A s s , b ‫؍‬ 7.6393(5) A s s , c ‫؍‬ 8.4191(6) A s s , ‫؍‬ 104.602(1)°°, V ‫؍‬ 1319.7(2) A

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## Abstract Two 2D Anderson polyoxomolybdate‐based compounds, [{Ni(H~2~O)~4~}~2~{Ni(OH)~6~Mo~6~O~18~}]·4H~2~O (1) and [Ni(H~2~O)~6~][Ag~2~{Ni(OH)~6~Mo~6~O~18~}]·8H~2~O (2), were synthesized and characterized by elemental analysis, IR spectroscopy, SEM, and single‐crystal XRD. Their thermal behavior

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