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Hydrogen storage in solar produced single-walled carbon nanotubes

✍ Scribed by D Luxembourg; G Flamant; A Guillot; D Laplaze


Publisher
Elsevier Science
Year
2004
Tongue
English
Weight
375 KB
Volume
108
Category
Article
ISSN
0921-5107

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✦ Synopsis


Single-walled carbon nanotube samples were synthesized with solar energy. The products are characterized by electron microscopy, Raman spectroscopy and nitrogen isotherms. The maximum value of the hydrogen uptake is 1 wt.% at 253 K and 6 MPa. The results are discussed by taking account of the structure and the BET surface of the samples. The hydrogen capacity is not proportional to the BET surface in these samples and does not seem to be linked to the amount of SWNT.


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Single walled carbon nanotubes (SWCNTs) dispersed in 2-propanol are deposited on the alumina substrate using drop cast method. The deposited SWCNTs are characterized using the techniques SEM, EDS and FTIR. Then the SWCNTs are functionalized with BH 3 using LiBH 4 as the precursor. FTIR, XPS and CHNS