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HREM, TEM and XRD observation of nanocrystalline phases in TiO2 obtained by the sol-gel method

✍ Scribed by A.M. Tonejc; A. Turković; M. Gotić; S. Musić; M. Vuković; R. Trojko; A. Tonejc

Book ID: 117358159
Publisher: Elsevier Science
Year: 1997
Tongue: English
Weight: 378 KB
Volume: 31
Category: Article
ISSN: 0167-577X
DOI: 10.1016/s0167-577x(96)00257-1

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## Abstract TiO~2~ powders were synthesized by a sol–gel method from tetrabutyl orthotitanate solution in the presence of water and hydrochloric acid. In order to study the effect of water content and hydrolysis catalyst (HCl) on crystal structure of the TiO~2~, a composition of H~2~O:EtOH:HCl was