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Highly enantioselective synthesis of terutroban key intermediate via asymmetric hydrogenation

โœ Scribed by Maj, Anna M.; Suisse, Isabelle; Pinault, Nathalie; Agbossou-Niedercorn, Francine

Book ID
122192899
Publisher
Elsevier Science
Year
2014
Tongue
English
Weight
618 KB
Volume
17
Category
Article
ISSN
1631-0748

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โœ Zhicong Geng; Yun Wu; Shifeng Miao; Zongxuan Shen; Yawen Zhang ๐Ÿ“‚ Article ๐Ÿ“… 2011 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 364 KB

A series of optically active b-hydroxy sulfonamides were synthesized for the first time by asymmetric transfer hydrogenation of the corresponding b-ketosulfonamides using the Ru-TsDPEN-HCOOH-Et 3 N catalytic system, in excellent yields (up to 95%) with excellent diastereo-(up to > 99:1 dr) and enant