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High Yield Synthesis, Separation and Structural Characterization of New [N + N]-Polyazamacrocycles.

✍ Scribed by Markus Allmendinger; Philipp Zell; Amal Amin; Ulf Thewalt; Martti Klinga; Bernhard Rieger


Publisher
John Wiley and Sons
Year
2003
Weight
79 KB
Volume
34
Category
Article
ISSN
0931-7597

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A new copper(II) tetrazolate coordination polymer [Cu(pzta) 2 ] n (1) (pzta=5-pyrazinyltetrazolate) was prepared from the hydrothermal reaction of Cu(OAc) 2 β€’H 2 O with NaN 3 and pyrazinecarbonitrile (pzCN) in the presence of ethanol, and characterized by elemental analysis, IR, TGA and X-ray crysta