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High-yield nitration of benzene in the synthesis of 15N-labelled nitrobenzene, acetanilide, and diphenylamine

✍ Scribed by Raymond J. Konior; Ling Yang; Robert I. Walter

Publisher
John Wiley and Sons
Year
1990
Tongue
French
Weight
160 KB
Volume
28
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Labelled H^15^NO~3~ was used as the least‐cost source of nitrogen label to prepare nitrobenzene by reaction of acetyl nitrate with excess benzene. This labelled product was subsequently converted to acetanilide‐^15^N and diphenylamine‐^15^N.

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