𝔖 Bobbio Scriptorium
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High surface area silica xerogels produced using triethoxysilane under non-supercritical conditions. Molecular hydrogen proposed as the high surface area promoter

✍ Scribed by Prof. James M. Tour; Cynthia M. Kafka


Book ID
101412887
Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
342 KB
Volume
5
Category
Article
ISSN
0935-9648

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✦ Synopsis


added to the solution dropwise over one minute. The solution was stirred overnight at room temperature. After filtration and removal of the solvent under reduced pressure, the residue was flash chromatographed on silica gel. Elution with dichloromethane/petroleum ether (1 : 1) gave, after removing the solvent, an orange solid which was recrystallized from dichloromethane/hexane