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High sensitivity measurement of amino acid isotope enrichment using liquid chromatography–mass spectrometry

✍ Scribed by Hans M.H. van Eijk; Karolina A.P. Wijnands; Babs A.F.M. Bessems; Steven W. Olde Damink; Cornelis H.C. Dejong; Martijn Poeze

Book ID
119289252
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
865 KB
Volume
905
Category
Article
ISSN
1873-376X

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## Abstract The sensitivity of high‐precision liquid chromatography/combustion isotope ratio mass spectrometry (LC/C‐IRMS) was improved by more than two orders of magnitude by modifications which permit optimization of flows. The lower limits for high precision are about 3 μg of analyte on‐column f