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High-Resolution NMR Probe for Experiments at High Pressures

✍ Scribed by L. Ballard; C. Reiner; J. Jonas

Publisher: Elsevier Science
Year: 1996
Tongue: English
Weight: 136 KB
Volume: 123
Category: Article
ISSN: 1064-1858
DOI: 10.1006/jmra.1996.0216

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✦ Synopsis

A 300 MHz high-resolution, high-pressure NMR probe which operates in the pressure range of 1 bar to 9 kbar at temperatures of -30 to 100°C is described. Specialized novel design features of the probe are discussed and test spectra showing resolution better than 1 Hz (<3.0 x 10(-9)) for 8 mm samples are presented. Potential biochemical applications of this probe are illustrated by experiments dealing with the pressure-induced unfolding of hen egg white lysozyme.

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