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High resolution MAS-NMR of quadrupolar nuclei in powders

✍ Scribed by A Samoson; E Kundla; E Lippmaa

Publisher
Elsevier Science
Year
1982
Weight
407 KB
Volume
49
Category
Article
ISSN
0022-2364

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πŸ“œ SIMILAR VOLUMES

Satellite transition high-resolution NMR
Satellite transition high-resolution NMR of quadrupolar nuclei in powders
✍ A. Samoson πŸ“‚ Article πŸ“… 1985 πŸ› Elsevier Science 🌐 English βš– 296 KB

Relative shif= of the central and satellite lransllion lines determine :he precrsc iosotropic chemical shlfls of I = 5/2 and 9/2 quadrupolar nuclei in solids The sarelhle transition is conveniently measured through the nxatron sidebands.

High-resolution multiple quantum MAS NMR
High-resolution multiple quantum MAS NMR spectroscopy of half-integer quadrupolar nuclei
✍ Gang Wu; David Rovnyank; Boqin Sun; Robert G. Griffin πŸ“‚ Article πŸ“… 1996 πŸ› Elsevier Science 🌐 English βš– 500 KB

We demonstrate the utility of a two-pulse sequence in obtaining high-resolution solid state NMR spectra of half-integer quadrupolar nuclei with magic-angle-spinning (MAS). The experiment, which utilizes multiple/single-quantum correlation, was first described in a different form by Frydman and Harwo