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High-resolution 1H NMR in solids with multiple-pulse sequences and magic-angle sample spinning at 270 MHz

โœ Scribed by G Scheler; U Haubenreisser; H Rosenberger


Publisher
Elsevier Science
Year
1981
Weight
675 KB
Volume
44
Category
Article
ISSN
0022-2364

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High-resolution 1H NMR spectroscopy in r
โœ Jian Zhi Hu; Donald N. Rommereim; Robert A. Wind ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 309 KB ๐Ÿ‘ 1 views

It is demonstrated that a high-resolution (1)H NMR spectrum of excised rat liver can be obtained using the technique of magic angle turning (MAT) at a sample spinning rate of 1 Hz. A variant of the phase-corrected MAT (PHORMAT) pulse sequence that includes a water suppression segment was developed f