A sampling system for high resolution gas-liquid chromatography, based on the dynamic solvent effect, is described. Volatiles areaccumulated off -line in a concentrator/injector and delivered to the column using an on-line inlet. Volatiles may be accumulated from gaseous or liquid matrices; they may
β¦ LIBER β¦
High precision trace analysis in capillary gas-liquid chromatography using an inlet based on the static solvent effect
β Scribed by Lawson, K. H. ;Pretorius, V. ;Apps, P. J.
- Publisher
- John Wiley and Sons
- Year
- 1987
- Tongue
- English
- Weight
- 365 KB
- Volume
- 10
- Category
- Article
- ISSN
- 0935-6304
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β¦ Synopsis
A sample inlet, based on the static solvent effect has been designed and constructed. The inlet can handle samples up to 20 1-11 which allows for the detection, using an F.I.D., of constituents in the parts per billion range. The reproducibility of the inlet in terms of peak percentage area is around 1% relative standard deviation over a range of chemical types.
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