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High-Accuracy Residual 1 H N − 13 C and 1 H N − 1 H N Dipolar Couplings in Perdeuterated Proteins

✍ Scribed by Meier, Sebastian; Häussinger, Daniel; Jensen, Pernille; Rogowski, Marco; Grzesiek, Stephan

Book ID: 127052570
Publisher: American Chemical Society
Year: 2003
Tongue: English
Weight: 64 KB
Volume: 125
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja028740q

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## Abstract The cyclodipeptides cyclo(L‐alanyl‐L‐phenylalanyl) and cyclo(D‐alanyl‐L‐phenylalanyl) were synthesized with various atoms substituted by the isotopes ^15^N and ^13^C. Thus, the coupling constants ^15^N–^1^H, ^13^C–^1^H, and ^13^C–^15^N could be obtained, in addition to the commonly used