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Heptacoordinated vanadium: Preparation and structure of hexacarbonyl(trimethylstannio)vanadium (Sn—V)

✍ Scribed by Gerhard E. Herberich; Lars Wesemann; Ulli Englert

Publisher
Springer
Year
1993
Tongue
English
Weight
297 KB
Volume
4
Category
Article
ISSN
1040-0400

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Graphite intercalation compounds (GIC) of vanadium fluoride have been prepared in a fluorine atmosphere. The GICs prepared from highly oriented pyrolytic graphite (HOPG) were stage l-8 compounds with composition, &\_B,VF,,,\_,,. The apparent size of intercalated VF;(d,) decreased from 5.33 A to 4.15