𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Headspace solid-phase microextraction for characterization of fragrances of lemon verbena (Aloysia triphylla) by gas chromatography-mass spectrometry

✍ Scribed by Nam-Sun Kim; Dong-Sun Lee


Publisher
John Wiley and Sons
Year
2004
Tongue
English
Weight
323 KB
Volume
27
Category
Article
ISSN
1615-9306

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

Natural fragrances from lemon verbena (Aloysia triphylla) were studied by headspace solid phase microextraction (HS‐SPME) techniques followed by gas chromatography‐mass spectrometry (GC‐MS), with six different fibre coatings being tested to evaluate the extraction efficiencies of several selected compounds. A total of 14 compounds were identified in the fragrances of lemon verbena. Geranial and neral were detected as major components and α‐pinene, β‐pinene, β‐caryophyllene, and curcumene as minor components. Enantiomeric analysis of chiral compounds from lemon verbena was carried out on a chiral column. α‐Pinene, limonene, and camphor in the fragrances emitted from lemon verbena were found in the (+), (–), and (–) forms, respectively.


📜 SIMILAR VOLUMES


Speciation of inorganic and tetramethylt
✍ Nikolaos M. Tzollas; George A. Zachariadis 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 180 KB

## Abstract A headspace solid‐phase microextraction (HS‐SPME) method coupled to GC‐MS was developed in order to determine trace levels of tetramethyltin (TeMT) and inorganic tin (iSn) after ethylation to tetraethyltin (TeET) in various matrices. The derivatization of iSn and the extraction of both

Headspace solid-phase microextraction wi
✍ Jiping Ma; Ronghui Xiao; Jinhua Li; Jie Li; Benzhang Shi; Yanjuan Liang; Wenhui 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 English ⚖ 313 KB 👁 1 views

## Abstract A simple, fast, sensitive and cost‐effective method based on headspace solid‐phase microextraction (HS‐SPME) with on‐fiber derivatization coupled with gas chromatography–mass spectrometry was developed for the determination of six typical aldehydes, 2__E__‐hexenal, heptanal, 2__E__‐hept

Characterization of the volatile profile
✍ Riccardo Romoli; Maria Cristiana Papaleo; Donatella de Pascale; Maria Luisa Tuti 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 English ⚖ 392 KB

Bacteria belonging to the __Burkholderia cepacia__ complex (Bcc) are significant pathogens in Cystic Fibrosis (CF) patients and are resistant to a plethora of antibiotics. In this context, microorganisms from Antarctica are interesting because they produce antimicrobial compounds inhibiting the grow