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Group 3 Metal Complexes of Salen-like Fluorous Dialkoxy−Diimino Ligands: Synthesis, Structure, and Application in Ring-Opening Polymerization of rac -Lactide and rac -β-Butyrolactone

✍ Scribed by Grunova, Ekaterina; Kirillov, Evgueni; Roisnel, Thierry; Carpentier, Jean-François

Book ID: 118745183
Publisher: American Chemical Society
Year: 2008
Tongue: English
Weight: 252 KB
Volume: 27
Category: Article
ISSN: 0276-7333
DOI: 10.1021/om800611c

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The reaction of one equivalent of dilithiated O(SiMe 2 -Ap-H) 2 Cl(THF) Bu 4 N (5), O(SiMe 2 -Ap) 2 Y(BH 4 ) 2 Na(THF) 2 (6) and O(SiMe 2 -Ap) 2 Y(CH(TMS) 2 ) 2 Li(THF) 3 ( ), respectively. The [Ap-H = -N(2-amino-4-methylpyridine)] (1), generated in situ, with LnCl 3 (Ln = Y, Sm) in THF affords O(Si