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Grignard Synthesis of 2-Phenyl-2-butanol in Optically Active Solvents

✍ Scribed by ALLENTOFF, NORMAL; WRIGHT, GEORGE F

Book ID
126899908
Publisher
American Chemical Society
Year
1957
Tongue
English
Weight
806 KB
Volume
22
Category
Article
ISSN
0022-3263

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## ABSTRACT Enantioselective syntheses of two stereoisomers of 3‐hydroxy‐4‐phenyl‐2‐butanone were investigated via Shi's asymmetric epoxidation or Sharpless asymmetric dihydroxylation of silyl enol ether. (__R__)‐3‐Hydroxy‐4‐phenyl‐2‐butanone was obtained in 73% enantiomeric excess (__ee__) by Shi'