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Green synthesis of 5-substituted-1,3,4-thiadiazole-2-thiols as new potent nitrification inhibitors

✍ Scribed by Ajoy Saha; Rajesh Kumar; Rajendra Kumar; C. Devakumar

Publisher
Journal of Heterocyclic Chemistry
Year
2010
Tongue
English
Weight
213 KB
Volume
47
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

magnified image A fast, efficient synthesis of 5‐substituted‐1,3,4‐thiadiazole‐2‐thiols was successfully developed, assessed using green chemistry matrices, and compounds were screened for their in vitro nitrification inhibitory activity. The greener method was superior with higher energy efficiency, E(nvironmental) factor, atom economy, atom efficiency, carbon efficiency, and reaction mass efficiency. J. Heterocyclic Chem., (2010).

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## Abstract magnified image One‐stage synthesis of 5‐substituted (alkyl, aryl, heteroaryl, arylalkyl, heteroalkyl, alkoxy‐, aryloxy)‐2‐(2,4‐dihydroxyphenyl)‐1,3,4‐thiadiazoles is described. The compounds were prepared by the reaction of sulfinyl‐bis(2,4‐dihydroxythiobenzoyl) (STB) with hydrazides