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Grafting of [Cu(NCCH3)6][B{C6H3(m-CF3)2}4]2 on the surface of aminosilane modified SBA-15

✍ Scribed by Ayyamperumal Sakthivel; Ahmed K. Hijazi; Akef I. Al Hmaideen; Fritz E. Kühn

Book ID: 104055441
Publisher: Elsevier Science
Year: 2006
Tongue: English
Weight: 350 KB
Volume: 96
Category: Article
ISSN: 1387-1811
DOI: 10.1016/j.micromeso.2006.07.009

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✦ Synopsis

A copper complex with weakly coordinating anions is grafted on the surface of mesoporous SBA-15 molecular sieves through an aminosilane linker. The nature of the support after the grafting is examined by powder XRD, TEM and N 2 adsorption/desorption analysis. Elemental analysis, FT-IR, TG-MS and MAS-NMR studies confirm the successful grafting of the complexes on the surface. The grafted material is applied as catalysts for aldehyde olefination.

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