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Gradient, High Resolution, Magic Angle Sample Spinning NMR

✍ Scribed by Maas, W. E.; Laukien, F. H.; Cory, D. G.


Book ID
127301677
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
77 KB
Volume
118
Category
Article
ISSN
0002-7863

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Rotor Synchronization of Radiofrequency
✍ Jean-Michel Wieruszeski; GΓ©rard Montagne; Gianni Chessari; Pierre Rousselot-Pail πŸ“‚ Article πŸ“… 2001 πŸ› Elsevier Science 🌐 English βš– 161 KB

We have investigated the extent to which rotor synchronization of radiofrequency pulses leads to spectral improvement in highresolution magic angle spinning NMR experiments. Several pulse sequences were tested, and the effect was found to be maximal in homonuclear TOCSY spectra. The physicochemical