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Gel permeation chromatography of poly(styrene-co-divinylbenzene) microgels. Effect of electrolyte concentration in the solvent system dimethylformamide plus lithium bromide

✍ Scribed by C. Booth; J.-L. Forget; I. Georgii; W.S. Li; C. Price


Publisher
Elsevier Science
Year
1980
Tongue
English
Weight
255 KB
Volume
16
Category
Article
ISSN
0014-3057

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✦ Synopsis


Tightly crosslinked poly(styrene-co-divinylbenzene) microgels with molecular weights in the range 10T-10 s g mol-1 have been dissolved in dimethylformamide containing LiBr and investigated by gel permeation chromatography and viscometry. The effect of LiBr concentration on the elution volume in GPC can be explained in terms of a diffuse double layer. The product [~]M adequately describes the separation in GPC provided that the LiBr concentration is high and adsorption is absent.