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GC–MS analysis of low-molecular-weight dicarboxylic acids in atmospheric aerosol: comparison between silylation and esterification derivatization procedures

✍ Scribed by Maria Chiara Pietrogrande; Dimitri Bacco; Mattia Mercuriali


Book ID
105892761
Publisher
Springer
Year
2009
Tongue
English
Weight
191 KB
Volume
396
Category
Article
ISSN
1618-2650

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## Abstract Three derivatization agents used in GC analysis of amino acids were compared: __N,O__‐bis(trimethylsilyl)trifluoroacetamide, (BSTFA), __N__‐methyl‐__N__‐(__tert__‐butyldimethylsilyl)trifluoroacetamide (MTBSTFA), and isobutyl chloroformate (iBuCF). It was shown that the analytical charac