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Gas chromatography of dimethylalkylsilyl ether derivatives of bile acid methyl esters

✍ Scribed by Akemi Fukunaga; Yoshio Hatta; Masataka Ishibashi; Hiroshi Miyazaki

Book ID
108334889
Publisher
Elsevier Science
Year
1980
Tongue
English
Weight
729 KB
Volume
190
Category
Article
ISSN
1873-3778

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Bile acids, such as cholic, chenodeoxycholic, deoxycholic, lithocholic and ursodeoxycholic acids, were allowed to react with hexafluoroisopropanol and trifiuoroacetic anhydride at 37" for 30 min. The resulting derivatives were gas chromatographed on QF-1, with flame ionization detection, and were id